CARETECH OXILYSERШUser Manual
钝化膜检测仪使用手册INTRODUCTION介绍
With the Oxilyser3you can measure the surface quality of stainless steel alloys in a reliable and accurate way.The measuring principle is based upon rest potential measurement of the stainless steel surface in a specially developed electrolyte.Minor surface activity will be indicated directly.After several years of scientific research, supported by the European Commission,the Oxilyser was successfully introduced to the world market in1992,succeeded by the Oxilyser2in2004and the Oxilyser3in 2009.Since2018the Oxilyser3and it's technology are owned and manufactured by Marine Care.
使用钝化膜检测仪，可以可靠和准确地测量不锈钢合金的表面质量。测量原理是：基于在特殊研发的电解液中不锈钢表面剩余电位的测量。表面微小的活动将被仪器直接显示出来。经过欧盟委员会几年的科学研究，钝化膜检测仪于1992年成功引入世界市场，通过2004年的第二代和2009年的第三代逐渐被大众认可。自2018年以来，第三代钝化膜检测仪和它的技术逐渐由海洋管理公司掌控和制造。APPLICATIONS应用领域
The most important applications of the Oxilyser3are:
1.Check surface passivity before,during and after the pickling and/or passivation treatment.
2.Check of the surface passivity after contact with a corrosive substance succeeded by rinsing of the surface.During the rinsing the surface will renew its passive layer within4-24hours.
3.Check the surface passivity of storage and transport tanks after cleaning and prior to loading them with corrosive substances such as orange juice or chemicals.
钝化膜检测仪最重要的应用是：
1.检查不锈钢表面在酸洗和/或钝化处理之前、期间和之后的钝化膜。
2.检查不锈钢表面与腐蚀性物质接触清水冲洗后的钝化膜，冲洗过程中，不锈钢表面将在4-24小时内生成钝化膜。
3.检查不锈钢储运罐清洗后，装载橙汁或化学品等腐蚀性物质前的钝化膜。The Oxilyser3is not a corrosion measuring instrument.It will not react properly on weld discoloration or already visible corroded surfaces.The Oxilyser only works reliably on surfaces that are clean.The first quality control for a stainless steel surface is a visual check.
钝化膜检测仪不是一种腐蚀测量仪器，它在焊接变或明显具有腐蚀的表面无法精确检测，只能在清洁干净的不锈钢表面上才能可靠地工作。一般来说，不锈钢表面质量检查的首要手段就是目视检查。
INSTRUMENT DESCRIPTION仪器描述
The Oxilyser is switched ON by choosing the proper alloy-group with a rotary switch. After switching on,the LCD display will show a slight negative value,this has no meaning.The same for the LED,which will be red after switching the instrument ON. The delivery includes a reference electrode with black cable and a red'anode clamp' with red cable.During the measuring,over a scale from0-100,a'passivity signal will be generated.The LED will automatically change from red to green after reaching an acceptable passivity signal.The acceptance level depends on the alloy group that has been selected with the rotary switch.
打开钝化膜检测仪，通过旋转开关选择合适的不锈钢等级。打开后，液晶显示屏显示少量负值，LED灯呈红，此情况是正常现象，不代表任何意义。仪器附件包括一个带黑电缆的参考电极和一个带红电缆的红“阳极夹”。在测量过程中，读数显示在0-100的读数时，就表明产生了“钝化膜信号”。在达到合格的钝化膜信号时，LED将自动从红变为绿。验收等级取决于通过旋转开关选择的不锈钢等级，不一样的不锈钢等级验收标准有所不同
BATTERY电池
A battery symbol in the LCD displays indicates LOW BATTERY.For changing the battery unscrew the
Lid and loose the battery clip from the old battery,replacing it with a new 9V battery.Preferably use Alkaline batteries
液晶显示器中的电池符号表示电池不足。如果要更换电池，请打开盖子，松开旧电池上的电池夹，更换为新的9V电池。优选地使用碱性电池REFERENCE ELECTRODE参考电极
The reference electrode has been made of plastic in order to make it suitable for industrial use.A reference electrode can only give a signal if the small ceramic membrane in the tip of the probe is in contact with a electrolyte and an anode.For that reason filter papers are being used as electrolyte bearer.After wetting the paper with electrolyte,it is placed on the surface and the tip of the reference electrode must be placed on top of this.The paper must be wetted thoroughly to ensure good contact of the membrane with the surface!If the reference electrode gives no signal, it could be blocked with an air bubble against the ceramic membrane on the inside of the electrode.In that case,shake the bubble out with short strong strokes in one direction.
参考电极由塑料制成，为了更适合工业用途。参考电极只有在探针尖端的小陶瓷膜与电解质和阳极接触时才能发出信号。因此，滤纸被用作电解质载体。用电解质润湿滤纸后，将其放置在待测不锈钢表面，将参考电极的尖端放置在纸上。纸张必须彻底湿润，以确保探针尖端膜片与待测表面的良好接触！
如果参考电极不发出信号，它可能是被气泡阻挡在电极内部的陶瓷膜上。在这种情况下，朝一个方向强力甩掉泡沫。
A long life time of the reference electrode is best guaranteed when the ceramic membrane is in contact with a potassium chloride solution.We recommend to always fill the plastic cap with a drop of potassium chloride and place it on the tip of the probe.During the measurement,the tip of the reference electrode must have been cleaned thoroughly with D.l.water and a clean tissue.
当参考电极的陶瓷膜与氯化钾溶液保持接触时，可以保证其使用寿命。我们建议在探针顶端的塑料盖中注入一滴氯化钾存放，以延长使用寿命。在但测量时，必须用去离子水水和干净的纸巾彻底将参考电极的尖端清洗干净。ELECTROLYTE STAINLESS STEEL不锈钢电解质
The electrolyte'stainless steel'is based upon an acetic acid solution.It is unharmful and not flammable or explosive.Nevertheless it is not suitable for internal use and we recommend to wash hands after contact with the fluid and to clean spilled fluid immediately.
Further,the electrolyte contains a small but well balanced quantity of salts.In order not to contaminate the electrolyte during the measurement,the tip of the reference electrode must be clean as well as the measuring surface and the filter papers.For that reason keep the lid on the filter paper box.
“不锈钢”电解质是以冰醋酸溶液为基础的。它无害，不易燃或易爆。但它不适合内部使用，我们建议在接触该液体后立即洗手，如有泄漏，立即用清水冲洗。此外，电解质中含有少量且均衡的盐分。为了在测量过程中不污染电解质，参比电极的尖端以及测量表面和滤纸都必须保持干净。并且保持盖子干净无污染。How TO DO THE MEASUREMENT如何进行测量
On the other side of this manual chart,you find a stepwise manual on how to do the measurement.Prior to measuring it must be known which alloy is going to be measured(0%Molybdenum,2%Molybdenum or6%Molybdenum/duplex stainless steel).
在本手册图的反面，您可以到关于如何逐步执行测量。在测量前，必须要知道测量哪种不锈钢（0%钼/304、2%钼/316L或6%钼/双相不锈钢）。MAINTENANCE AND CALIBRATION维护和校准
The Oxilyser3does not require maintenance apart from a bi-yearly calibration and keeping it clean.Please keep the Oxilyser and its case free of chemicals and dust.We recommend a calibration once every2years.Depending on the way of use,the lifetime of the battery is2-5years
钝化膜检测仪不需要维护，除了两年一次校准并保持其清洁就可以。请保持钝化膜检测仪及其箱子中没有化学物质和灰尘。我们建议每两年进行一次校准。根据使用方式，电池的使用寿命为2-5年
表面）
Electrolyte'stainless steel)
0+40
不锈钢电解液
0+15 Electrolyte stainless
steel>2year tenability不reference group
锈钢电解液>2年保质期
*If necessary,cool surface with cold water and dry it.
必要时，用冷水冷却表面并干燥。
Electronics电子器件：
-Measurement of rest potential.-静止电位的测量。
-Impedance resistance>10MOhm.-阻抗电阻>10莫姆。
TROUBLE SHOOTING问题解答
Passivity value on LCD remains around zero
-Check the contacts
-Be sure that the filter paper has been sufficiently wetted with electrolyte and that the tip of the reference electrode is in contact with the fluid.
-Check if a transparent coating was applied on the surface.
-Check if surface is clean and free of iron
-Check the reference electrode.Is there an air bubble in the tip?Shake the air bubble out with strong short strokes in one direction.
如若液晶显示屏上的钝化膜数值保持在零左右，可检查以下因素：
-检查接触面
-确保滤纸已被电解液充分湿润，并且参考电极的尖端与电解液接触。
-检查表面是否涂上了透明涂层。
-检查表面是否干净且无铁质
-检查参考电极。尖端是否有气泡？如果有，朝一个方向强力的摇晃掉气泡。
INSTRUCTIONS FOR USE使用说明:
1.The first quality control of a stainless surface is a visual inspection.The Oxilyser3 measures effectively on clean surfaces.The measuring surface must be clean and dry. The Oxilyser3might not indicate property on surface defects such as clearly visible weld colorings or scaling on the surface
不锈钢表面的首先质量控制是目视检查。检测仪只有在清洁的表面上才能够有效地测量，因此测量表面必须是清洁和干燥。但检测仪可能不能检测出表面缺陷的性质，如清晰可见的焊接着或表面的结垢
2.Connect the reference electrode to the black connector and the anode or contact clamp to the red connector.Remove the transparent plastic cap from the tip of the reference electrode.Clean the tip of the reference electrode properly with D.l.water and a tissue.
将参考电极连接到黑连接器，并将阳极或触点夹连接到红连接器。从参比电极的尖端取下透明的塑料盖。用去离子水及纸巾正确清洁参考电极的尖端。3.Switch the instrument on by selecting the correct alloy group.
OMo/304means all austenitic stainless steels with<0,5%Mo.Examples are AISI304,304L,321,Wst.Nr.1.4306,1.4541and Wst.Nr.1.4301.
2Mo/316stands for all austenitic stainless steels with2-3%Mo.Examples are AlSI316,316L,316Ti,Wst.Nr.1.4571,1.4404,1.4432,1.4435.
6Mo/duplex stands for all stainless steels with4-8%Mo and duplex stainless steels Examples are254SMO,6hMo,duplex2205,duplex2507and AISI904L
打开仪器，选择正确的不锈钢材质栏。
OMo/304：表示所有钼含量<0.5%的奥氏体不锈钢。例如AISI304、304L、321、Wst.Nr.1.4306、1.4541和Wst.Nr.1.4301.
2Mo/316：代表所有钼含在2-3%范围内的奥氏体不锈钢。例如AlSI316、316L、316Ti、Wst.Nr.1.4571,1.4404,1.4432,1.4435.
6Mo/双不锈钢：代表所有钼含量在4-8%范围内不锈钢，双不锈钢有254SMO、6hMo、双2205、双2507和AISI904L
4.Wet a filter paper strip with electrolyte'stainless steel'and place the paper on the stainless steel surface as well as the reference electrode tip on the properly wetted paper.The ceramic membrane in the tip must contact the fluid properly.If necessary, add an extra drip of fluid to the tip.
用“不锈钢”电解质浸湿滤纸条，将纸放在不锈钢表面，并将参考电极尖端放在适当湿润的纸上。尖端的陶瓷膜必须正确地接触到液体。如有必要，请在其尖端多滴一滴液体。
5.In general,the LCD value will rapidly increase to a value well above50,the LED will change to green.The LED must stay green,which means that the LCD value should not drop significantly during
the measurement
一般来说，LCD值将迅速增加到远高于50，LED将变为绿。LED必须保持绿，并且在测量过程中LCD值不应显著下降才能视为合格
6.Whether the LCD value will start to decrease again,will be clear within10 seconds.If the value decreases,it may not fall back in the'red area'again.
液晶显示屏值是否会再次开始下降，将在10秒内显现，如果该值下降，可能不会再次回落到“红区域”。
7.After use:fill the transparent cap of the electrode with a few drops of the potassium chloride to avoid it drying out when not in use.Store all components in the Oxilyser3case
使用后：用几滴氯化钾填充电极的透明盖，以避免其在不使用时干燥。将所有组件都装进钝化膜检测仪的箱子中，避免丢失。
Stable value(or value varies slightly up and down）；↑=Value rises；↓=Value falls.
代表稳定值（或稳定值略有上下变化）；↑代表值上升；↓代表值下降。
·
The LED switches from red to green at value55for0%Mo alloys,60for2%Mo alloys and65for6%Mo and duplex stainless steels.This is valid for a temperature of 18℃.At other temperatures,the switch limit red/green can differ slightly.
LED在值为55时从红切换为绿（0%钼含量合金），2%钼含量合金为60,6%Mo 和双链不锈钢为65，在温度为18℃有效。在其他温度下，开关变红/绿的数值可能略有不同。
·The best passivity has been achieved if the value is higher than respectively55,60 or65and the value remains STABLE.
如果该值分别高于55、60或65，且该值保持稳定，则达到最佳的钝化膜·Stable values up to90are possible.If a value after20seconds still is unstable and goes down,the passivity is not good.In that case normally the LED will be RED. Normally a measurement takes3-10seconds
稳定的读数值也有可能超过90。如果20秒后数值仍然不稳定并下降，则钝化膜不好。在这种情况下，LED通常会是红的。一般情况下，通常一次测量需要3-10秒
·If a surface has been pickled,grinded or blasted recently,it will be ACTIVE.This means that the surface needs time to passivate.Dependent on the alloy quality, temperature and presence of moist(rinsing water)this takes4-24hours.
如果表面最近被酸洗、打磨或喷砂，表面是活跃的。这意味着表面需要时间来钝化。根据不锈钢质量、温度和潮湿（冲洗水）的环境，需要4-24小时。
·If a surface has been contacted with a corrosive fluid during longer time,it might have been activated,which means that corrosion can start.Cleaning this surface after, e.g.unloading a storage or transport tank,will allow a renewed passivation.The

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